Deliberate Force: Aug.- Sept. 1994:

On 28 February 1994 4 Bosnian-Serb Soko G-4 Super Galebs were destroyed by two F-16C's. One of the F-16's (USAF 89-2137 / RS) shot down 3 !! Super Galebs, 2 with the AIM-9M Sidewinder, and the third with an AIM-120 AMRAAM. The second F-16 (USAF 89-2009 / RS) downed the 4th aircraft with an AIM-9M Sidewinder missile.

Allied Force: 24 March - 10 June 1999:

On 24 March 1999: a Royal Netherlands Air Force F-16AM (J-063) shot down a Serbian MiG-29 Fulcrum using an AIM-120B AMRAAM missile. This became the first air to air kill in Allied Force.

Source

http://www.zap16.com/mil%20fact/f-16.htm